Liang Taomao, Wang Fengyu, Zhang Chaoda, Xie Baohua, Xu Xiaoyi. Experimental study on separating ilmenite from a tailing of vanadium-bearing titanomagnetite ore in Panxi region[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(2): 103-108. doi: 10.7513/j.issn.1004-7638.2021.02.018
Citation:
Liang Taomao, Wang Fengyu, Zhang Chaoda, Xie Baohua, Xu Xiaoyi. Experimental study on separating ilmenite from a tailing of vanadium-bearing titanomagnetite ore in Panxi region[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(2): 103-108. doi: 10.7513/j.issn.1004-7638.2021.02.018
Liang Taomao, Wang Fengyu, Zhang Chaoda, Xie Baohua, Xu Xiaoyi. Experimental study on separating ilmenite from a tailing of vanadium-bearing titanomagnetite ore in Panxi region[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(2): 103-108. doi: 10.7513/j.issn.1004-7638.2021.02.018
Citation:
Liang Taomao, Wang Fengyu, Zhang Chaoda, Xie Baohua, Xu Xiaoyi. Experimental study on separating ilmenite from a tailing of vanadium-bearing titanomagnetite ore in Panxi region[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(2): 103-108. doi: 10.7513/j.issn.1004-7638.2021.02.018
A vanadium-bearing titanomagnetite dressing tailing in Panxi region contents of 8.25% TiO2. In the ore, the main valuable mineral was ilmenite, and the main gangue minerals were augite and hornblende, and the gangue minerals are of stronger magnetism. Both the particle size and disseminated grain size of ilmenite are relatively fine in the ore, the fine fraction of −38 μm reaches 45.46% and contributes 49.79% TiO2. In order to utilize the titanium resources effectively, a dressing test for recovering ilmenite was carried out. In this paper, the ore was graded into two parts by particle size after the strong magnetite minerals were removed by a drum magnetic separator, then the coarse-grained ore was separated by using spiral chute and the fine-grained ore was separated by using a ZQS high-gradient magnetic separator. A comprehensive ilmenite concentrate with a yield rate of 36.45%, a TiO2 grade of 15.88% and a recovery of 70.11% was obtained. Sulfuric acid and sodium silicate were used as regulators and YTB-1 as a collector to separate ilmenite from the comprehensive concentrate which was desulphurized by flotation beforehand. After one rougher stage, four finer stages, and one scavenging stage, the medium ore are returned in sequence, and finally, an ilmenite concentrate with a yield of 9.57%, a TiO2 grade of 47.23% and a recovery of 54.79% was obtained. Ilmenite mineral resource was recovered effectively.
Shao Juan. Application and development of titanium alloys[J]. Rare Metals and Cemented Carbides, 2007,(4):61−65. (邵娟. 钛合金及其应用研究进展[J]. 稀有金属与硬质合金, 2007,(4):61−65. doi: 10.3969/j.issn.1004-0536.2007.04.015
[2]
Wu Jianxin. Application of titanium alloys in marine materials[J]. Marine Equipment/Materials & Marketing, 2020,(8):5−6. (吴建新. 钛合金材料在船舶材料上的应用[J]. 船舶物资与市场, 2020,(8):5−6.
[3]
Gong Jiazhu. Technical progress of titanium dioxide manufacturing processes[J]. Inorganic Chemicals Industry, 2012,44(8):1−4. (龚家竹. 钛白粉生产工艺技术进展[J]. 无机盐工业, 2012,44(8):1−4. doi: 10.3969/j.issn.1006-4990.2012.08.001
[4]
Chong Xiaoxiao, Luan Wenlou, Wang Fengxiang, et al. Overview of global titanium resources status and titanium consumption trend in China[J]. Conservation and Utilization of Mineral Resources, 2020,40(2):162−170. (崇霄霄, 栾文楼, 王丰翔, 等. 全球钛资源现状概述及我国钛消费趋势[J]. 矿产保护与利用, 2020,40(2):162−170.
[5]
Sun Renbin, Wang Qiushu, Yuan Chunhua, et al. Analysis of global titanium resources situation[J]. China Mining Magazine, 2019,28(6):1−6, 12. (孙仁斌, 王秋舒, 元春华, 等. 全球钛资源形势分析[J]. 中国矿业, 2019,28(6):1−6, 12.
[6]
Wang Hongbin, Meng Changchun. New process to recover coarse ilmenite in Midi titanium concentration plant of Panzhihua[J]. Mining and Metallurgical Engineering, 2011,31(4):51−54. (王洪彬, 孟长春. 攀枝花密地选钛厂粗粒钛铁矿回收新工艺研究[J]. 矿冶工程, 2011,31(4):51−54. doi: 10.3969/j.issn.0253-6099.2011.04.014
[7]
Wang Fengyu, Yang Zhaojun, Luo Rongfei, et al. Recovery increase of −38 μm ultra fine ilmenite using ZQS high gradient magnetic separator[J]. Metal Mine, 2019,(8):93−97. (王丰雨, 杨招君, 罗荣飞, 等. 采用ZQS高梯度磁选机提高超细粒级(−38 μm)钛铁矿回收效果[J]. 金属矿山, 2019,(8):93−97.
Figure 1. Flow chart of low-intensity magnetic separation by using vertical ring wet high-gradient magnetic separator
Figure 2. Flow chart of low-intensity magnetic separation–desliming–spiral sluice separation–ZQS recovering fine ilmenite by using high-gradient magnetic separator
Figure 3. Flow chart of ilmenite flotation
Figure 4. Influence of dosage of sulfuric acid on the flotation of ilmenite
Figure 5. Influence of dosage of collector YTB-1 on the flotation of ilmenite
Figure 6. Influence of dosage of water glass on the flotation of ilmenite
Figure 7. Flow chart of the whole closed-circuit process