Volume 44 Issue 5
Oct.  2023
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Yin Yanchao, Li Longteng, Lü Yifan, Sun Zhijie, Yu Wei, Jiang Peng. Effect of post heat treatment on the microstructure and properties of as-annealed Ti75 alloy[J]. IRON STEEL VANADIUM TITANIUM, 2023, 44(5): 68-75. doi: 10.7513/j.issn.1004-7638.2023.05.011
Citation: Yin Yanchao, Li Longteng, Lü Yifan, Sun Zhijie, Yu Wei, Jiang Peng. Effect of post heat treatment on the microstructure and properties of as-annealed Ti75 alloy[J]. IRON STEEL VANADIUM TITANIUM, 2023, 44(5): 68-75. doi: 10.7513/j.issn.1004-7638.2023.05.011

Effect of post heat treatment on the microstructure and properties of as-annealed Ti75 alloy

doi: 10.7513/j.issn.1004-7638.2023.05.011
  • Received Date: 2023-03-07
    Available Online: 2023-11-04
  • Publish Date: 2023-10-31
  • In order to study the effect of post heat treatment on the properties of annealed Ti75 alloy, different post treatment conditions including annealing temperatures and cooling rates were selected to treat the annealed Ti75 alloy. The microstructure evolution was analyzed by OM and SEM, and the influence of microstructure on tensile properties and impact toughness of Ti75 alloy was studied. The results show that the volume fraction of equiaxed α phase has no obvious change when alloy is annealed at low temperature. When the annealing temperature is high enough, the equiaxed α phase begins to dissolve and its volume fraction decreases gradually with the increase of temperature. The evolution of strength and impact toughness of annealed Ti75 alloy after air cooling by different annealing temperature at 750 - 950 ℃ is basically the same as that of furnace cooling. The yield strength and tensile strength decrease firstly, then increase a little and then decrease again with the increase of temperature. The main reason for strength increasing is that a large number of fine α phases exists in the β transformation matrix structure which are difficult to deform. The impact toughness has no obvious change when alloy is annealed at low temperature region and then increases with the increase of temperature. The strength of annealed Ti75 alloy after annealing and air cooling is higher than that of furnace cooling. The impact toughness of annealed Ti75 alloy after annealing at low temperature region and air cooling is higher than that of furnace cooling, while at the high temperature region it shows the opposite changing tendency.
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  • [1]
    Hai Minna, Huang Fan, Wang Yongmei. Brief analysis of the application of titanium and titanium alloy in marine equipment[J]. Metal World, 2021,(5):16−21. (海敏娜, 黄帆, 王永梅. 浅析钛及钛合金在海洋装备上的应用[J]. 金属世界, 2021,(5):16−21.

    Hai Minna, Huang Fan, Wang Yongmei. Brief analysis of the application of titanium and titanium alloy in marine equipment[J]. Metal World, 2021, (5): 16-21.
    [2]
    Gorynin I V. Titanium alloy for marine application[J]. Materials Science and Engineering A, 1999,263(2):112−116. doi: 10.1016/S0921-5093(98)01180-0
    [3]
    Christoph Leyens, Manfred Peters. Titanium and titanium alloys: Fundamentals and application[M]. Weinheim: Wiley, 2003.
    [4]
    常辉, 廖志谦, 王向东. 海洋工程钛金属材料[M]. 北京: 化学工业出版社, 2017.

    Chang Hui, Liao Zhiqian, Wang Xiangdong. Titanium alloys for marine applications[M]. Beijing: Chemical Industry Press, 2017.
    [5]
    Yin Yanchao, Liu Jia, Zhang Shuaifeng, et al. Influence of aging treatment on microstructure and mechanical properties of Ti75 titanium alloy[J]. Titanium Industry Progress, 2023,40(1):21−26. (尹艳超, 刘甲, 张帅锋, 等. 时效工艺对Ti75合金显微组织及力学性能的影响[J]. 钛工业进展, 2023,40(1):21−26.

    Yin Yanchao, Liu Jia, Zhang Shuaifeng, et al. Influence of aging treatment on microstructure and mechanical properties of Ti75 titanium alloy[J]. Titanium Industry Progress, 2023, 40(1): 21-26.
    [6]
    Jiang Peng, Wang Qi, Zhang Binbin, et al. Application of titanium alloy materials for the pressure-resistant structure of deep diving equipment[J]. Strategic Study of CAE, 2019,21(6):95−101. (蒋鹏, 王启, 张斌斌, 等. 深海装备耐压结构用钛合金材料应用研究[J]. 中国工程科学, 2019,21(6):95−101. doi: 10.15302/J-SSCAE-2019.06.018

    Jiang Peng, Wang Qi, Zhang Binbin, et al. Application of titanium alloy materials for the pressure-resistant structure of deep diving equipment[J]. Strategic Study of CAE, 2019, 21 (6): 95-101. doi: 10.15302/J-SSCAE-2019.06.018
    [7]
    Yin Yanchao, Zhang Shuaifeng, Xu Yali, et al. Influence of pre-strain on deformation behavior of TC4 ELI titanium alloy[J]. Development and Application of Materials, 2023,38(1):66−72. (尹艳超, 张帅锋, 许亚利, 等. 预应变对TC4 ELI钛合金变形行为的影响[J]. 材料开发与应用, 2023,38(1):66−72.

    Yin Yanchao, Zhang Shuaifeng, Xu Yali, et al. Influence of pre-strain on deformation behavior of TC4 ELI titanium alloy[J]. Development and Application of Materials, 2023, 38(1): 66-72.
    [8]
    Liu Hongyan, Xu Xirong, Cai Na. Research on the forming process of Ti75 alloy head[J]. World Nonferrous Metals, 2019,(12):7−8. (刘鸿彦, 徐曦荣, 蔡娜. Ti75合金封头成形工艺研究[J]. 世界有色金属, 2019,(12):7−8.

    Liu Hongyan, Xu Xirong, Cai Na. Research on the forming process of Ti75 alloy head[J]. World Nonferrous Metals, 2019(12): 7-8.
    [9]
    Zhangjing, Song Dejun, Zhu Qiang, et al. Orthogonal finite element simulation of Ti75 tube bending at high temperature[J]. Transactions of Materials and Heat Treatment, 2020,41(6):190−196. (张静, 宋德军, 朱强, 等. Ti75管材高温弯曲成形的正交有限元模拟[J]. 材料热处理学报, 2020,41(6):190−196.

    Zhangjing, Song Dejun, Zhu Qiang, et al. Orthogonal finite element simulation of Ti75 tube bending at high temperature[J]. Transactions of Materials and Heat Treatment, 2020, 41(6): 190-196.
    [10]
    Cao Shouqi, He Xin, Liu Wanrong, et al. Study on laser welding technology and properties of Ti75 titanium alloy[J]. Journal of Physics: Conference Series, 2020,1622:012046. doi: 10.1088/1742-6596/1622/1/012046
    [11]
    Ji Dawei, Liu Yinqi, Chen Tao, et al. Research on the anisotropy of tensile properties and impact toughness of Ti75 alloy plate[J]. Development and Application of Materials, 2016,31(5):53−58. (纪大伟, 刘茵琪, 陈涛, 等. Ti75合金板材拉伸性能和冲击韧性各向异性的研究[J]. 材料开发与应用, 2016,31(5):53−58.

    Ji Dawei, Liu Yinqi, Chen Tao, et al. Research on the anisotropy of tensile properties and impact toughness of Ti75 alloy plate[J]. Development and Application of Materials, 2016, 31(5): 53-58.
    [12]
    Xie Yingjie, Fu Wenjie, Wang Ruining, et al. Effect of heat treatment on microstructure and mechanical properties of TA15 plates[J]. Titanium Industry Progress, 2013,30(6):26−29. (谢英杰, 付文杰, 王蕊宁, 等. 热处理对TA15钛合金中厚板材组织及力学性能的影响[J]. 钛工业进展, 2013,30(6):26−29.

    Xie Yingjie, Fu Wenjie, Wang Ruining, et al. Effect of heat treatment on microstructure and mechanical properties of TA15 plates[J]. Titanium Industry Progress, 2013, 30(6): 26-29.
    [13]
    Huang Sensen, Ma Yingjie, Zhang Shilin, et al. Influence of alloying elements partitioning behaviors on the microstructure and mechanical properties[J]. Acta Metallurgica Sinica, 2019,55(6):741−750. (黄森森, 马英杰, 张仕林, 等. α+β两相钛合金元素再分配行为及其对显微组织和力学性能的影响[J]. 金属学报, 2019,55(6):741−750.

    Huang Sensen, Ma Yingjie, Zhang Shilin, et al. Influence of alloying elements partitioning behaviors on the microstructure and mechanical properties[J]. Acta Metallurgica Sinica, 2019, 55(6): 741-750.
    [14]
    Zhang Zhenxuan, Lei Wen, Zhu Hong, et al. Effect of solution temperature and cooling rate on microstructure and mechanical properties of TC21 titanium alloy[J]. Hot Working Technology, 2016,45(8):217−220. (张珍宣, 雷雯, 朱红, 等. 固溶温度和冷却速率对TC21钛合金组织和力学性能的影响[J]. 热加工工艺, 2016,45(8):217−220.

    Zhang Zhenxuan, Lei Wen, Zhu Hong, et al. Effect of solution temperature and cooling rate on microstructure and mechanical properties of TC21 titanium alloy[J]. Hot Working Technology, 2016, 45(8): 217-220.
    [15]
    潘金生, 仝健民, 田民波. 材料科学基础[M]. 北京: 清华大学出版社, 2011.

    Pan Jinsheng, Tong Jianmin, Tian Minbo. Fundamentals of materials science[M]. Beijing: Tsinghua University Press, 2011.
    [16]
    Lütjering G. Influence of processing on microstructure and mechanical properties of (α+β) titanium alloys[J]. Materials Science and Engineering, 1998,A243:32−45.
    [17]
    Gerd L, James C Williams. Titanium[M]. Berlin: Springer-Verlag, 2007.
    [18]
    Yan Chong, Tilak Bhattacharjee, Jangho Yi, et al. Achieving bi-lamellar microstructure with both high tensile strength and large ductility in Ti-6Al-4V alloy by novel thermomechanical processing[J]. Materiallia, 2019: 100479.
    [19]
    赵永庆, 陈永楠, 张学敏, 等. 钛合金相变及热处理[M]. 长沙: 中南大学出版社, 2012.

    Zhao Yongqing, Chen Yongnan, Zhang Xuemin, et al. Phase transformation and heat treatment of titanium alloys[M]. Changsha: Central South University Press, 2012.
    [20]
    M F Savage, J Tatalovich, M J Mills. Anisotropy in the room-temperature deformation of α-β colonies in titanium alloys: role of the α-β interface[J]. Philosophical Magazine, 2007,84(11):1127−1154.
    [21]
    郑修麟. 材料的力学性能[M]. 西安: 西北工业大学出版社, 2009.

    Zheng Xiulin. Mechanical properties of materials[M]. Xi, an: Northwestern Polytechnical University Press, 2009.
    [22]
    Niinomi M, Kobayashi T. Toughness and microstructural factors of Ti-6Al-4V alloy[J]. Materials Science and Engineering, 1988,100:45−55. doi: 10.1016/0025-5416(88)90238-8
    [23]
    Niinomi M, Kobayashi T. Fracture characteristics analysis related to the microstructures in titanium alloys[J]. Materials Science and Engineering, 1996,A212:16−24.
    [24]
    Christophe Buirettea, Julitte Hueza, Nathalie Geyb, et al. Study of crack propagation mechanisms during charpy impact toughness tests on both equiaxed and lamellar microstructures of Ti-6Al-4V titanium alloy[J]. Materials Science and Engineering, 2014,A618:546−557.
    [25]
    Xu Jianwei, Zeng Weidong, Zhao Yawei, et al. Effect of microstructure evolution of the lamellar alpha on impact toughness in a two-phase titanium alloy[J]. Materials Science & Engineering, 2016,A676:434−440.
    [26]
    Li Shikai, Hui Songxiao, Ye Wenjun, et al. Effect of cooling rate on the microstructure and properties of TA15 ELI alloy[J]. Rare Metal Materials and Engineering, 2007,36(5):786−789. (李士凯, 惠松骁, 叶文君, 等. 冷却速度对TA15 ELI合金组织与性能的影响[J]. 稀有金属材料与工程, 2007,36(5):786−789.

    Li Shikai, Hui Songxiao, Ye Wenjun, et al. Effect of cooling rate on the microstructure and properties of TA15 ELI alloy[J]. Rare Metal Materials and Engineering, 2007, 36(5): 786-789.
    [27]
    Lei Lei, Zhao Yongqing, Zhao Qinyang, et al. Impact toughness and deformation modes of Ti-6Al-4V alloy with different microstructures[J]. Materials Science & Engineering, 2021,A801:140411.
    [28]
    Liu Rui, Hui Songxiao, Ye Wenjun, et al. Effects of cooling rate on dynamic fracture toughness for TC4 titanium alloy[J]. The Chinese Journal of Nonferrous Metals, 2010,20(1):691−694. (刘睿, 惠松骁, 叶文君, 等. 冷却速度对TC4钛合金动态断裂韧性的影响[J]. 中国有色金属学报, 2010,20(1):691−694.

    Liu Rui, Hui Songxiao, Ye Wenjun, et al. Effects of cooling rate on dynamic fracture toughness for TC4 titanium alloy[J]. The Chinese Journal of Nonferrous Metals, 2010, 20(1): 691-694.
    [29]
    Yang Zhijun, Guo Aihong, Wu Yizhou. Microstructure evolution of Ti6321 titanium alloy during annealing treatment and its effect on impact toughness[J]. The Chinese Journal of Nonferrous Metals, 2013,23(1):512−516. (杨治军, 郭爱红, 吴义舟. Ti6321钛合金退火处理过程中组织演变及其对冲击韧性的影响[J]. 中国有色金属学报, 2013,23(1):512−516.

    Yang Zhijun, Guo Aihong, Wu Yizhou. Microstructure evolution of Ti6321 titanium alloy during annealing treatment and its effect on impact toughness[J]. The Chinese Journal of Nonferrous Metals, 2013, 23(1): 512-516.
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