Controllable preparation of titanium dioxide nanotubes on titanium foil

Fan Xingping; Ma Lan; Yang Cheng; Fan Wei

doi:10.7513/j.issn.1004-7638.2021.06.016

Volume 42 Issue 6

Dec. 2021

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Fan Xingping, Ma Lan, Yang Cheng, Fan Wei. Controllable preparation of titanium dioxide nanotubes on titanium foil[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(6): 115-119. doi: 10.7513/j.issn.1004-7638.2021.06.016

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Fan Xingping, Ma Lan, Yang Cheng, Fan Wei. Controllable preparation of titanium dioxide nanotubes on titanium foil[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(6): 115-119. doi: 10.7513/j.issn.1004-7638.2021.06.016

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Controllable preparation of titanium dioxide nanotubes on titanium foil

doi: 10.7513/j.issn.1004-7638.2021.06.016

Fan Xingping^{1, 2
,},
Ma Lan^{1, 2},
Yang Cheng¹,
Fan Wei¹

1.
Panzhihua University, Panzhihua 617000, Sichuan, China
2.
Sichuan Key Laboratory of Vanadium and Titanium Resources Comprehensive Utilization, Panzhihua 617000, Sichuan, China

Received Date: 2021-07-21
Publish Date: 2021-12-31

Abstract

Abstract

Titanium dioxide nanotubes were prepared on the surface of titanium foil by electrochemical anodization. The diameter and wall size of the nanotubes were controlled by adjusting the anodizing voltage and time. The morphology of TiO₂ nanotube arrays was observed by scanning electron microscope (SEM) under different preparation conditions. The effects of anodizing voltage and time on the morphology of TiO₂ nanotube arrays were investigated. The crystal of TiO₂ nanotubes was adjusted by heat treatment and characterized by X-ray diffraction (XRD). The results showed that the orderly TiO₂ nanotubes were obtained at 40 V for 30 min in glycol aqueous solution containing 0.5% ammonium fluoride as electrolyte. After heat treatment at 450 ℃ for 2 h, the crystal of TiO₂ nanotubes has changed from amorphous into anatase, and a small part of the nanotubes collapsed.
- titania nanotube,
- titanium foil,
- anodic oxidation,
- voltage,
- oxidation time

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References(15)

References

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