Study on TiC/SiC reinforcement material by spark plasma sintering

Liu Xiaohong; Wang Yanfeng; Cao Yongdi; Liu Jianxiu; Wang Bingwei

doi:10.7513/j.issn.1004-7638.2021.06.022

Volume 42 Issue 6

Dec. 2021

Turn off MathJax

Article Contents

Article Navigation > IRON STEEL VANADIUM TITANIUM > 2021 > 42(6): 153-157

Liu Xiaohong, Wang Yanfeng, Cao Yongdi, Liu Jianxiu, Wang Bingwei. Study on TiC/SiC reinforcement material by spark plasma sintering[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(6): 153-157. doi: 10.7513/j.issn.1004-7638.2021.06.022

Citation:

Liu Xiaohong, Wang Yanfeng, Cao Yongdi, Liu Jianxiu, Wang Bingwei. Study on TiC/SiC reinforcement material by spark plasma sintering[J]. IRON STEEL VANADIUM TITANIUM, 2021, 42(6): 153-157. doi: 10.7513/j.issn.1004-7638.2021.06.022

Citation:

PDF( 982 KB)

Study on TiC/SiC reinforcement material by spark plasma sintering

doi: 10.7513/j.issn.1004-7638.2021.06.022

1.
Yellow River Conservancy Technical Institute, Kaifeng 475000, Henan, China
2.
Zhengzhou University of Light Industry, Zhengzhou 450000, Henan, China

Received Date: 2021-05-12
Publish Date: 2021-12-31

Abstract

Abstract

Mechanical reinforcement materials were prepared by spark plasma sintering (SPS), using SiC nanopowder and TiC particles as raw materials. The composite samples with different SiC content were characterized by SEM, and the composite sample with 10% SiC was tested by XRD. The effects of SiC content on the fracture toughness, conductivity, density and hardness of the composites were discussed. The results show that the grains are refined in the TiC/SiC reinforcement samples with lower structural defects and excellent compatibility between SiC and TiC. The component content in the sample with 10% SiC coincides well with the XRD analysis result. Compared with those of the pure TiC material, the fracture strength of the sample with 30% SiC is increased by about 116% and the average conductivity is enhanced by about 100 times. At the TiC/SiC ratio of 1.3∶1, the maximum value of density (4.3 g/cm³) and hardness (68.3HRA) can be obtained. The experimental results is consistent with the expected goals.
- SiC/TiC reinforced material,
- spark plasma sintering,
- fracture toughness,
- conductivity,
- hardness,
- wear resistance

FullText(HTML)

References(12)

References

[1]	Dai Peiyun, Zhou Ping, Wang Mibao, et al. Research progress of silicon carbide compact density materials[J]. China Ceramics, 2012,48(4):1−7. (戴培赟, 周平, 王泌宝, 等. 碳化硅致密陶瓷材料研究进展[J]. 中国陶瓷, 2012,48(4):1−7.
[2]	Wang Feifeng, Zhang Peihong, Gao Mingze. Research on the dielectric characteristics of nano-SiC/silicone rubber composites[J]. Journal of Harbin University of Science and Technology, 2015,20(3):82−85. (王飞凤, 张沛红, 高铭泽. 纳米碳化硅/硅橡胶复合物介电性研究[J]. 哈尔滨理工大学学报, 2015,20(3):82−85.
[3]	Liu Ping^, an, Zeng Lingke, Shui Anze, et al. Progress in preparation and application of ultrafine TiC powder[J]. Ordnance Materials Science and Engineering, 2006,29(5):82−85. (刘平安, 曾令可, 税安泽, 等. 超细碳化钛粉体的制备及应用研究进展[J]. 兵器材料科学与工程, 2006,29(5):82−85. doi: 10.3969/j.issn.1004-244X.2006.05.024
[4]	Xie Zhen, Zhou Dali, Yang Weizhong, et al. Preparation of nano-TiC powders by in-situ carbothermal method in vacuum[J]. Iron Steel Vanadium Titanium, 2017,38(1):38−42. (谢真, 周大利, 杨为中, 等. 真空原位碳热还原法制备纳米碳化钛粉末[J]. 钢铁钒钛, 2017,38(1):38−42. doi: 10.7513/j.issn.1004-7638.2017.01.007
[5]	Liu Yang, Zeng Lingke, Hu Xiaoli, et al. Progress in preparation and application of TiC[J]. China Ceramics, 2002,38(5):7−10. (刘阳, 曾令可, 胡晓力, 等. 碳化钛的合成及其应用研究进展[J]. 中国陶瓷, 2002,38(5):7−10. doi: 10.3969/j.issn.1001-9642.2002.05.003
[6]	Wang Guanzhong, Zhang Mingtao, Guo Pingyi. Research on Co-Mn composites material prepared by spark plasma sintering(SPS) process[J]. Powder Metallurgy Industry, 2014,24(6):28−32. (王冠仲, 张名涛, 郭平义. 放电等离子烧结法(SPS)制备Co-Mn复合材料的研究[J]. 粉末冶金工业, 2014,24(6):28−32.
[7]	Zhou Houxing, Zhou Ningsheng, Sun Jialin, et al. Preparation of single phase MgAlON material by spark plasma sintering[J]. Refractory Matter, 2002,36(3):128−131. (周厚兴, 周宁生, 孙加林, 等. 放电等离子烧结合成单相MgAlON材料[J]. 耐火材料, 2002,36(3):128−131. doi: 10.3969/j.issn.1001-1935.2002.03.002
[8]	Wang Xiufen, Zhou Xiya. Spark plasma sintering technology[J]. China Ceramics, 2006,42(7):14−16. (王秀芬, 周曦亚. 放电等离子烧结技术[J]. 中国陶瓷, 2006,42(7):14−16. doi: 10.3969/j.issn.1001-9642.2006.07.005
[9]	Gan Zuoteng, Ren Shubin, Shen Xiaoyu, et al. Research on diamond/Cu composites fabricated by spark plasma sintering[J]. Materials Science and Engineering Powder Metallurgy, 2010,15(1):59−64. (淦作腾, 任淑彬, 沈晓宇, 等. 放电等离子烧结法制备金刚石/Cu复合材料[J]. 粉末冶金材料科学与工程, 2010,15(1):59−64. doi: 10.3969/j.issn.1673-0224.2010.01.011
[10]	Yang Xinling, Wang Zichen, Li Fangni, et al. Microstructure and properties of silicon carbide/graphite composite ceramic seals[J]. Journal of the Chinese Ceramic Society, 2015,43(12):1686−1691. (杨新领, 王子晨, 李芳妮, 等. 碳化硅/石墨复合陶瓷密封材料的显微结构与性能[J]. 硅酸盐学报, 2015,43(12):1686−1691.
[11]	Gao Ying, Li Lanlan. Measuring resistivity of silicon wafers with four-point probe method and evaluation of uncertainty in measurement[J]. Materials Science, 2019,9(12):1041−1047. (高英, 李兰兰. 直排四探针法测量硅片电阻率及不确定度评定[J]. 材料科学, 2019,9(12):1041−1047.
[12]	Wang Feifeng, Zhang Peihong, Gao Mingze. Research on nonlinear conductivity characteristics of nano-SiC/silicone rubber compound[J]. Journal of Physics, 2014,63(21):1−8. (王飞凤, 张沛红, 高铭泽. 纳米碳化硅/硅橡胶复合物非线性电导特性研究[J]. 物理学报, 2014,63(21):1−8.