Technology Research on Dispersity of Titanium Dioxide
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摘要: 研究了TiO2颗粒"打浆分散-砂磨"组合工艺分散技术。采用黏度和粒度表征TiO2颗粒的分散状况,通过透射电镜观察分散前后TiO2颗粒大小和形貌的变化情况。探讨了分散剂种类、分散剂加量、砂磨介质粒径和砂磨时间对TiO2颗粒分散效果的影响。结果表明,TiO2颗粒的最佳分散工艺为:硅酸钠作为分散剂,添加量为TiO2质量分数的0.2%,采用粒径为0.4μm的氧化锆珠砂磨25 min,平均粒径为265 nm,粒度大小均匀,分散效果稳定。Abstract: The "dispersing and grinding"combined process was studied for dispersing TiO2.The dispersity of TiO2 particles was characterized as viscosity and particle size.The particle size and morphology of TiO2 before and after dispersing were observed using TEM.Effects of the dispersing agents and their addition amount,the size of grinding medium and grinding time on the dispersion of TiO2 were discussed.The results show that the optimum process conditions for dispersing TiO2 are as follows:sodium metasilicate as the dispersing agent with addition amount of 0.2%(mass ratio) for TiO2,ZrO2 as grinding medium with size of 0.4 μm and 25 min of the grinding time.The average particle size of TiO2 obtained under the optimum conditions is 265 nm with uniform particle size distribution and steady dispersing effect.
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Key words:
- titanium dioxide /
- dispersion /
- particle size /
- viscosity
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