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电子束选区熔化增材制造TiAl合金及其热处理工艺研究进展

王双赞 葛庚午 卢东 梁永锋 林均品

王双赞, 葛庚午, 卢东, 梁永锋, 林均品. 电子束选区熔化增材制造TiAl合金及其热处理工艺研究进展[J]. 钢铁钒钛, 2026, 47(1): 36-48. doi: 10.7513/j.issn.1004-7638.2026.01.005
引用本文: 王双赞, 葛庚午, 卢东, 梁永锋, 林均品. 电子束选区熔化增材制造TiAl合金及其热处理工艺研究进展[J]. 钢铁钒钛, 2026, 47(1): 36-48. doi: 10.7513/j.issn.1004-7638.2026.01.005
WANG Shuangzan, GE Gengwu, LU Dong, LIANG Yongfeng, LIN Junpin. Research progress on electron beam melting additive manufacturing of TiAl alloys and heat treatment processes[J]. IRON STEEL VANADIUM TITANIUM, 2026, 47(1): 36-48. doi: 10.7513/j.issn.1004-7638.2026.01.005
Citation: WANG Shuangzan, GE Gengwu, LU Dong, LIANG Yongfeng, LIN Junpin. Research progress on electron beam melting additive manufacturing of TiAl alloys and heat treatment processes[J]. IRON STEEL VANADIUM TITANIUM, 2026, 47(1): 36-48. doi: 10.7513/j.issn.1004-7638.2026.01.005

电子束选区熔化增材制造TiAl合金及其热处理工艺研究进展

doi: 10.7513/j.issn.1004-7638.2026.01.005
基金项目: 国家重点研发计划项目(2021YFB3700500);钒钛资源综合利用产业技术创新战略联盟资助项目(PGWX2023006)。
详细信息
    作者简介:

    王双赞,1999年出生,男,河南南阳人,博士研究生,研究方向为增材制造TiAl合金方面的基础研究,E-mail:wangshuangzan16@163.com

    通讯作者:

    梁永锋,1980年出生,陕西宝鸡人,博士,教授,研究方向为金属间化合物结构及功能材料,E-mail:liangyf@skl.ustb.edu.cn

  • 中图分类号: TF823

Research progress on electron beam melting additive manufacturing of TiAl alloys and heat treatment processes

  • 摘要: 电子束选区熔化技术(Electron Beam Melting,EBM)是增材制造脆性TiAl合金部件的理想成形方法,以实现TiAl合金复杂结构成形和优异性能。相较于其他增材制造方法,EBM具有预热温度高、不易开裂、氧含量低等优势,因而被广泛研究,尤其是Ti-48Al-2Cr-2Nb(4822)合金。EBM制备的4822合金平均晶粒尺寸通常小于20 μm,晶粒尺寸远小于传统铸造合金。EBM制备的4822合金室温强度最高可达600 MPa以上,但塑性较差且存在缺陷,热等静压(HIP)和高温热处理(HT)是提升力学性能重要的后处理手段,可将室温延伸率提升至1.3%。然而,EBM制备TiAl合金工艺及热处理还存在许多问题,综述了近年来EBM增材制造TiAl合金及其热处理工艺的研究进展,对目前存在的问题及应对措施进行了分析总结,并对增材制造TiAl合金未来的发展方向进行了展望。
  • 图  1  EBM结构示意和设备

    (a)结构示意[36];(b)EBM设备[37]

    Figure  1.  Schematic diagram and equipment of EBM

    图  2  EBM制备TiAl合金的显微组织演化和独特的显微组织形成示意[47]

    (a)EBM过程简要说明;(b)铺送粉末;(c)熔合多层;(d)铺送下一层粉末;(e)再次熔合多层

    Figure  2.  Schematic of microstructural evolution and the formation of unique layered microstructure in TiAl alloy fabricated by EBM[47]

    图  3  EBM制备TiAl合金的显微组织及电子束光斑尺寸、铝损失、硬度和孔隙率随散焦值的变化[50]

    (a)带状组织;(b)均匀组织;(c)电子束光斑尺寸(黑色)、铝损失(原子含量)(绿色)、硬度(红色)和孔隙率(橙色)随散焦值的变化

    Figure  3.  Microstructure of TiAl alloy prepared by EBM, and variations of the electron beam spot size, Al loss, hardness, and porosity with the FO[50]

    图  4  Ti-48Al-2Cr-2Nb合金打印态和热等静压后的内部缺陷变化[48]

    (a)打印态CT扫描结果;(b)热等静压态CT扫描结果

    Figure  4.  Changes in internal defects of Ti-48Al-2Cr-2Nb alloy in as-deposited and HIP[48]

    图  5  Ti-48Al-2Cr-2Nb合金打印态和热等静压态的显微组织及位错分布

    (a)打印态显微组织;(b)HIP态显微组织;(c)打印态位错分布;(d)HIP态位错分布(蓝色区域为无位错)[57]

    Figure  5.  Microstructures and dislocation distributions of the as-deposited and HIPed Ti-48Al-2Cr-2Nb alloy[57]

    图  6  两步热处理后Ti-48Al-2Cr-2Nb的显微组织[64]

    (a)低倍显微组织;(b)高倍显微组织

    Figure  6.  Microstructure of Ti-48Al-2Cr-2Nb after two-step heat treatment[64]

    图  7  退火+稳定化热处理后TNM-B1合金的显微组织[67]

    Figure  7.  Microstructure of TNM-B1 alloy after annealing and stabilization heat treatment[67]

    (a)(d) 1240 ℃-1 h+850 ℃/6 h; (b)(e)1400 ℃-15 min+850 ℃/6 h; (c)(f) 1400 ℃-15 min+ 1210 ℃-1 h+850 ℃/6 h

    图  8  热处理EBM TiAl-4822的拉伸性能[59]

    (a)屈服强度与温度的关系;(b)伸长率与温度的关系;(c)极限强度与温度的关系;(d)室温应力-应变曲线

    Figure  8.  Tensile properties of heat-treated EBM TiAl-4822[59]

    图  9  打印态和热处理态4822合金在800 ℃下的蠕变结果[62]

    应变-时间曲线:(a)打印态4822, (b)热处理态4822;速率-应变曲线:(c)打印态4822, (d)热处理态4822

    Figure  9.  Creep results of the as-printed and heat-treated 4822 alloy at 800 ℃[62]

    表  1  增材制造TiAl合金的室温及高温拉伸性能

    Table  1.   Room temperature and high-temperature tensile properties of additive manufactured TiAl alloys

    Alloy State Temperature/℃ UTS/MPa YS/MPa EL/% Refs
    4722 EBM RT 534~572 0.67~0.98 [65]
    EBM+HT RT 552~598 0.73~1.04
    4722 EBM RT 462~568 462~530 0.27~0.98 [41]
    4822 EBM+HIP RT 434 374 1.15 [36]
    EBM+HIP+HT RT 469 353 1.10
    4822 EBM RT 603±18 555±11 0.94±0.06 [71]
    4822 EBM+HIP+HT RT 429±26 372±13 0.8±0.2 [59]
    4822 EBM RT 695.29 [70]
    EBM 650 700±10 4.28
    4822 EBM 700 512.3±7.3 487.7±3.3 1.31±0.24 [72]
    4822 EBM+HIP+HT RT 474±23 382±11 1.3±0.3 [73]
    EBM+HIP+HT 800 460 2
    458 EBM RT 450~500 [74]
    EBM+HIP RT 600~800
    TNM-B1 EBM+HT 800 770 715 6 [67]
    Note: 4722 refers to Ti-47Al-2Cr-2Nb; 4822 refers to Ti-48Al-2Cr-2Nb; 458 refers to Ti-45Al-8Nb; TNM-B1 refers to Ti-43.5Al-4Nb-1Mo-0.1B; UTS denotes the ultimate tensile strength; YS denotes the yield strength; EL denotes the elongation.
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  • 收稿日期:  2025-03-20
  • 录用日期:  2025-04-07
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  • 网络出版日期:  2026-02-28
  • 刊出日期:  2026-02-28

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